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sample solution. The lter technique is also widely used in PIXE (particle induced X-ray emission), radioisotope X-ray analysis,3 and X-ray absorption spectroscopy using the X-ray uorescence yield method. The interaction between X-rays and matter is classi ed into absorption, elastic scattering, and inelastic scattering. The basic physical formula of X-ray absorption are described elsewhere.4 6 The physical constants, such as X-ray absorption coef cients or equivalently the imaginary part of the atomic scattering factor are listed elsewhere.4 9 The relation among the imaginary part of the atomic scattering factor, the imaginary part of the refractive index, the linear absorption coef cient, and the mass absorption coef cient, are concisely described in the literature.4,6,7 The measurement and interpretation of the X-ray absorption coef cients as the change of the X-ray energy are called the X-ray absorption spectrometry or spectroscopy. Since most of the materials analysis techniques using the X-ray absorption phenomena have already been described in the Encyclopedia of Analytical Chemistry 4 the present subchapter is devoted to the concise summary and addenda to the Encyclopedia. X-Ray absorption spectroscopy is referred to as XANES (X-ray absorption near edge structure) and EXAFS (extended X-ray absorption ne structure) (Figure 5.8.2).10 XANES refers to the ne structure about 50 eV around the edge. EXAFS is used for the oscillating ne structure from 50 to 1000 eV above the absorption edge. The Fourier transform of this EXAFS oscillation yields a

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