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Reactive comminution is a field of long tradition in human mankind, and a short history of mechanochemistry can be found in Refs [1 3] Very early applications are the lighting of fire with flint, pyrite and steel, the use of matches, the preparation of gunpowder, or the welding of silver and platinum in South America During the early 20th century, contributions from for example Tamman [4] extended the view on pressure-induced phase transformations and solid-state reactions The initiation of explosions during milling gave rise to the theory of hot spots in mechanical activated solids and liquids, as mentioned by Bowden and Yoffe [5] The mechanical activation of solids and mechanochemical reactions are a field of prolonged research which has been conducted since the classification of Ostwald [6, 7] and his findings about the so-called Ostwald ripening.

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Many small crystals form in a system initially but slowly disappear, except for a few that grow larger The formation of smaller crystals is kinetically favored and lowers the supersaturation of the solution The larger crystals are thermodynamically favored because of the smaller surface energy The morphology, structure and energy state of mechanically treated substances have been examined by many authors Thiessen et al [8], Schmalzried [9], and Heinicke et al [10] were among the first to compile these earlier studies into books about tribochemistry Boldyrev and Meyer [11], Heegn [12] and Tkacova [13] showed the positive influence of mechanical treatment on minerals and other materials Fundamental ideas about the description of mechanochemical reactions have also been presented by Heegn [14, 15] The theory of fracture mechanism and stressed single particles has been originated by Sch nert [16].

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The utilization of mechanical energy in solid transformations can be divided into four clusters: mechanical comminution: the size reduction of solids by mechanical means; mechanical activation: the use of mechanical energy to alter the behavior of solids in a subsequent process; mechanical alloying: the use of mechanical energy to cause dissolution or dispersion of different solid materials; and.

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The properties of detectors are discussed in Sec. 3.3.3. The noise produced in detectors of infrared radiation is usually of thermal origin. Today, the number of detectors operating at room temperature (Golay cell, thermocouple, pyroelectric detectors) is therefore decreasing. Thermoelectric coolers based on the Peltier effect are used for temperatures down to -30 "C. Liquid nitrogen (-196 "C), and sometimes even liquid helium (4 K ) are also employed. 'Closed cycle refrigerators' are usually not employed for cooling the detectors in analytical laboratories, since they may produce noise due to their mechanical vibrations. Cooled semiconductor quantum detectors (MCT, mercury-cadmium-telluride) have their advantageous low NEP only in a restricted wavelength range (Fig. 3.3-8). Therefore, several of these detectors are often combined in a spectrometer for alternative use. Semiconductor array detectors are gaining importance, especially in the NIR range. They can be used in special infrared spectrometers for process control. Some detectors employ the optothennal effect: the absorbed modulated infrared radiation heats the sample and its environment, thus producing sound waves which are recorded with a microphone. They can be combined with scanning spectrometers and interferometers. A Golay cell (Golay, 1949) measares the optothermal pressure change by a light beam which is deflected by a reflecting membrane. The first infrared process spectrometer, the URAS, already employed the absorption bands of a detector gas to specifically analyze the concentration of this particular gas in a sample. This is a non-dispersive spectrometer already mentioned in Sec. 1.

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