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the microphase-separated domains of azo-SCLCP (i.e., PAzoMA) act as crosslinks supporting the extension of PnBA chains. Since the physical cross-links are not formed by an amorphous polymer such as PS, but by a liquid crystalline and photosensitive polymer, new interesting properties can emerge from the coupled elasticity, liquid crystallinity, and photoactivity. In particular, as compared to conventional thermoplastic elastomers such as SBS, an intermediate state exists PB PS for PAzoMA-b-PnBA-b-PAzoMA between the normal elastic (Tg oToTg ) and PS thermoplastic (TWTg ) regimes. In other words, when stretched at TniWTWTg of azo-SCLCP (Tni is the nematic-to-isotropic phase transition temperature), a longrange orientation of azobenzene mesogens can be induced inside the deformed LC microdomains that can still support part of the elastic extension of PnBA chains. This molecular orientation of azobenzene can subsequently be retained in the relaxed lm at room temperature, resulting in thermoplastic elastomers containing glassy microdomains with oriented mesogens. However, despite the well-de ned structure of this type of ATE, its mechanical strength and deformability are not as good as azo-SCLCP-grafted SBS. This is the main reason for which azo-SCLCPgrafted SBS was utilized for the study of mechanical tunable diffraction gratings as described later.

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1 2 3 4 5 6 7 8 9 */ 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 #include <ncurses.h> #define MENUMAX 6 void drawmenu(int item) { int c; char mainmenu[] = Main Menu ; char menu[MENUMAX][21] = { Answer E-mail , Off to the Web , Word processing , Financial management , Maintenance , Shutdown }; clear(); addstr(mainmenu); for(c=0;c<MENUMAX;c++) { if( c==item ) attron(A_REVERSE); /* highlight selection */ mvaddstr(3+(c*2),20,menu[c]); attroff(A_REVERSE); /* remove highlight */ }

When a solution-cast lm of ATE is stretched at room temperature, the deformation gives rise to a long-range molecular orientation of azobenzene groups along the strain direction (SD), which can be switched between two orientational states upon alternating UV and visible light irradiation as a result of the coupled mechanical and optical effects. This orientational switching in a

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stretched lm can easily be detected by polarized infrared or UV Vis spectroscopy. Figure 11.5 shows an example of the reversible change in orientation of azobenzene mesogens in an ATE lm stretched to 500% deformation and, under strain, subjected to UV and visible light exposure, the order parameter being determined from the infrared dichroism (Bai and Zhao, 2001). Under unpolarized UV irradiation, the mechanically induced orientation can be erased because of the trans cis isomerization, while it is recovered upon unpolarized visible irradiation that drives the reverse cis trans isomerization. The switching is observed with eight cycles in two separate experiments differing in the irradiation time. Figure 11.6 schematically illustrates the main features of the coupling of mechanical and optical effects, where four different states of azobenzene groups in the lm are depicted, and for each state two polarized UV Vis spectra of the lm are shown (solid and dashed lines represent the polarization parallel and perpendicular to the SD, respectively). In the unstretched lm, 1, the elongated trans-azobenzene groups, whose maximum absorption is B360 nm, are in the LC phase but have no long-range orientation, as seen from the spectra displaying no dichroism. If the unstretched lm is exposed to UV light, the trans cis isomerization occurs, and the photochemical phase transition results in disordered cis-azobenzene groups (bent form), 2, absorbing at B450 nm and showing no dichroism. This process can be reversed by the cis trans back-isomerization of azobenzene either upon visible

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