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I hope this book will be a useful indoctrination for novice chemists making the transition from organic teaching laboratories to the synthetic chemistry research laboratory, either in academe or industry I also attempted to assemble some of the more useful but hard to locate information that the practicing synthetic chemist needs on a day-to-day basis My aspiration for this book is to nd it (with several tabbed pages) on chemists lab benches Finally, I aim to remind all readers of the little details about lab work that we may learn at some point in our careers but easily forget When you are vexed by a particularly challenging experiment, I hope that paging through this book is one approach you take to solving your problem of the day, and that it is concise enough to encourage you to do so.

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I organized the book to parallel the processes involved in planning, executing, and analyzing the synthetic preparation of a target molecule I included a new chapter not found in earlier books on this subject matter: an example of the different formats in which the synthesis of a known compound may be published I hope this chapter assists novice chemists in translating experimental descriptions into action items for today s experiment I also found on the Web many new and valuable electronic resources contributed by the community of synthetic chemists This book has been over 25 years in the making I rst learned of an effort to assist beginning experimental students in learning the ropes of research laboratory work while a postdoctoral fellow at Columbia in 1980 Clark Still was giving a mini-course to his students on how to work in the lab.

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