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in which n denotes the number of observations, y is the given (or true ) value of the constituent of interest and y the concentration predicted by the PLS model. Given a certain data set, the RMSE values are calculated for different numbers of components included in the PLS model. Normally the RMSE reduces with increasing number of PLS components until a minimum or constant value is reached and the corresponding number of components is regarded as optimal. The prediction error is composed of two contributions, the remaining interference error and the estimation error. The former is the systematic error due to unmodelled interference in the spectral data and the latter is caused by random measurement noise of various kinds or by

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to 20 pm are usually employed (Table 5.5), although some devices have been fabricated in thin SOI films as well.' - 117 It is also possible, using a mask during oxygen ion implantation, to produce SIMOX material with bulk regions (i.e., unimplanted areas). Using such a techr ique, it is possible to combine SOI CMOS devices and bulk power devices on a same chip. The flexibility of dielectric isolation allows for the fabrication of mixed chips featuring, such as CMOS + NPN bipolar + VDMOS devices (Fig. 5.36) using a process that requires fewer masking step than the equivalent bulk process.118 The main drawback of dielectric isolati on lies in the fact that it is accompanied by an increased thermal resistance between the device and the heat sink, because the thermal conductivity of SiO 2 is lowei than that of silicon. As a result, the temperature rise in SOI power devices is higher than that in bulk power devices. The differences in self-heating between SO and bulk power devices is largest for short power transients because the initial temperature rise in SOI devices is more rapid. As the pulse length increases, the difference in temperature rise between SOI and bulk devices converges to a constant value, which is proportional to the thickness of the buried oxide. For oxide thicknesses u ider 2 ltm, the steady-state temperature is

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The solvent properties of hydrazine on metal chalcogenides (especially sul des) have been previously considered, with little solubility noted for most systems examined.29 Hydrazine hydrate has been used as a medium to precipitate rst- and second-row transition metal sul des and selenides.30 The simple approach described in this chapter generally employs additional chalcogen (S, Se, Te) in anhydrous hydrazine to improve directly the solubility and lmforming properties of selected metal chalcogenides, including SnSe2 xSx, In2Se3, GeS2, GeSe2, Cu2S, Sb2Se3, Sb2Te3, CuInSe2, and Ga2Se3.31 38 Dissolution generally proceeds by formation of metal chalcogenide anions accompanied by hydrazinium cations. The additional chalcogen added to the hydrazine facilitates the disruption of the metal chalcogenide framework by breaking up M X M linkages, in analogy to the dimensional reduction examples described above. For ZnTe (and perhaps selected other metal tellurides), dissolution occurs through the breakdown of the 3D ZnTe structure into one-dimensional (1D) ZnTe chains separated by coordinated neutral molecules.34 The process of dimensional reduction is different for zinc telluride. However, the result on solubility is similar to the examples that involve salt formation. In many respects, hydrazine is an ideal solvent, since it is both a small and volatile molecule and also tends not to coordinate strongly.29,39 Hydrazine is, therefore, relatively easy to dissociate from the precursor at low temperature. In addition, the absence of carbon in the precursor and solvent implies that cleaner lm deposition may be possible after the heat treatment (i.e., absence of carbon impurities). Hydrazine is, however, also toxic and explosive and should therefore be used only with adequate protective measures in place to avoid contact with either the vapor or the liquid and/or ignition sources.40,41 3.3.1 SnSe2 xSx Films

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