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Download the PDF Combine software program and combine multiple PDF files to a single PDF file in few clicks. The purity of the crystallization product can be affected by the parameters that control any crystallization as well as the presence of other chemical species, including the starting materials, that can be occluded from the reaction mixture. The particle size distribution can be affected by supersaturation, reaction rate, mixing, and other factors that affect crystallization in general. The degree to which control of the crystallization must be of concern obviously depends on downstream processing. In some cases, physical attributes may not be signi cant and the reaction can be optimized on the basis of chemical kinetics alone. In other cases, however, the requirements for maximum selectivity may be different than those for physical attributes, requiring a trade-off in actual system design. An example of reaction-induced crystallization where the particle size and purity must be controlled is discussed in 17 (Example 17-3; Larson et al., 1995). In this case, mixing played a key role by balancing circulation with shear to achieve micromixing for the reaction but avoiding overmixing. This con guration achieves growth without shedding and/or crystal fracture. A key factor is the time of addition a mesomixing issue as well as a means of regulating supersaturation. Mixing can also play a key role in affecting the morphology of a crystalline product. This effect results from the complex interaction between the impeller and nucleation and growth. The reader is referred to the discussion on mixing and crystallization in 17. pdf merge online Merge PDF Files Online - Sejda
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